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GNR Analytical Instruments|X-Ray Fluorescence (XRF)

TX 2000

TXRF Analysis

Laboratory TXRF spectrometer for quantitative multi-element trace and ultra-trace analysis, with automatic primary-beam switching.

GNR TX 2000
Overview

About the TX 2000

An outstanding spectrometer that allows to perform Energy Dispersive X-Ray Fluorescence Analysis in Total Reflection Geometry.

TX 2000 is the state of the art laboratory spectrometer for quantitative multi element trace analysis using Total Reflection X-Ray Fluorescence (TXRF).

TXRF is a type of Energy Dispersive X-Ray Fluorescence (EDXRF) in which the beam strikes the sample, deposited as a thin layer on a carrier, at a very small incidence angle, in order to exploit enhancement given by the total reflection effect. As far as the sample is thin enough (thin film approximation), the tecnique’s main strenghts are:

TX 2000, equipped with an automatic primary beam switching system (MoKa, WLa/Lb and bremsstrahlung 33 keV), a Silicon Drift Detector (SDD) and an high power X-Ray Tube is the optimal solution for applications in environmental, chemicals and nuclear fields.

Key features
  • simultaneous multi-element analysis from Na to Pu
  • no matrix effect
  • no matrix-dependent calibration curves
  • improved detection limits (LOD) down to ng/g or lower
  • minimum amount of sample
  • microanalysis capabilities
  • Stepper motors with optical encoders ensure extremely precise angular values.
  • Enhanced excitation mode by selection of the most suitable monochromatized energy (W-La/W-Lb/Mo-Ka) provided by the combination of double anode MO/W X-ray tube and W/Si multilayer. Other X-Ray anodes can be monochromatized as well.
  • Peltier-cooled Silicon Drift Detector with an energy resolution better than of 133eV (FWHM@MnKa, 1ms peaking time)
  • Minimal distance between the sample and the detector (mounted to the axis normal to the plane of the sample).
  • Instrumental detection limits below ng/g.
  • Helium flux attachment to improve the detection limits for the light elements.
  • No matrix effect
Applications

Documented applications

  • Environmental Analysis: water, dust, sediments, aerosol (ISO/TS 18507:2015, ISO 20289:2018)
  • Medical/Pharma: toxic elements in biological fluids and tissue samples, catalyst residues
  • Forensic Science: analysis of extremely small sample quantities
  • Pure chemicals: acids, bases, salts, solvents, water, ultrapure reagents
  • Oils and greases: crude oil, essential oil, fuel oil, gasoline, jet fuel
  • Pigments: ink, oil paints, powder
  • Nuclear Industry: measurements of radioactive elements

Matrices, elements and ranges depend on the configuration supplied; EMUS confirms them in the quotation.

Industries

Sectors served

GNR application fields

Chemical & PetrochemicalClinicalEnvironmentMaterial SciencePharmaceutical
Specifications

Technical data

X-Ray Generator
Maximum Output Power
3 kW
Max Output Voltage
60 kV
Max Output Current
60 mA
Voltage Step Width
0.1 kV
Current Step Width
0.1 mA
X-Ray Tube
Type
Glass, Mo/W anode, long fine focus
Focus
0.4 x 12 mm
Max Output
2.5 kW
(*) Different anodes can be mounted on request
Multilayer monochromator
Type
W/Si
Reflectivity 80%
Excitation energies
W-La
8.4 keV (ΔE<1 keV)
W-Lb
9.67 keV (ΔE<1 keV)
Mo-Ka
17.44 keV (ΔE<1 keV)
Bremsstrahlung
33 keV
Sample Holder
12 position sample holder
Detector
Active area
40 mm2 as standard. (50 mm2 as option)
Energy resolution
≤ 133 eV FWHM @Mn-Ka (1 μs peaking time)
Atmosphere
Air or He Flux
Case
Dimensions
Width 580 mm, Height 1631.5 mm, Depth 793 mm
Weight
200 kg (without chiller)
Leakage X-Rays
< 1 mSv/Year (full safety shielding according to the international guidelines)
Cooling
External Chiller (1146h, 570w, 740d)

Reproduced from official GNR product information. Values apply to the configuration described by GNR; final configuration is confirmed in the EMUS quotation.

Software

Operating software

  • GNR proprietary software for T XRF supports several tasks of analysis, from Data Acquisition, having the full control of all the process and hardware settings (generator and tube, detector, measurements set up) to Data Analysis:
  • Least square Marquardt fit procedure for the area calculation (spectral analysis)
  • Automatic/manual search function
  • Manual or automatic calibration of energy
  • Quantification via an internal standard using theoretical and experimental sensitivity curves
Related products

Related GNR products

Manufacturer

GNR Analytical Instruments

TheTX 2000 is part of the GNR Analytical Instruments portfolio, supplied and supported by EMUS across the Balkan region.

Request Technical Consultation

Talk to an EMUS engineer about theTX 2000, your materials and the analytical configuration that fits your laboratory or production line.